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Bruker Fast Lane on automates (CMC-assit)
On Bruker automatic machines, it is possible to perform an automatized consistency analysis using the CMC-assist module.
For this, you have to proceed the following way :
1. Generate a mol file with your molecule.
2. Depose it in the "mol" server localized on nmr.epfl.ch
2.a for MAC :
- go somewhere free on your desktop and type cmd-K,
- then type the server address : smb://nmr.epfl.ch/mol,
- log into the window with your GASPAR data, you can now copy/delete whatever mol file in that
window.
- It will be available directly on the automate NMR.
2.b for PC :
- click on the Computer shortcut from your desktop or from the Start Menu.
- in the toolbar you will find several buttons, including one called Map network drive.
- click on it and the Map Network Drive window will open. Leave the automatically assigned drive
letter
and then type the folder you want to connect to. In our case \\nmr.epfl.ch\mol
- Click on Finish then double click on the new icon. d. If necessary, in the login window, type the
user
"intranet\GASPAR_USER" and your gaspar password (replace GASPAR_USER by your specific
one).
3. Go to the automate NMR, prepare your experiment in a classical way. Choose the experiment :
CMCQ_PROTON.
4. In the Consistency/structure item, add the link to your molecule like this : /sdb/mnt/mol/name.mol
(replace name.mol by the name of your file).
5. A complete report is available as a pdf file inside the pdata subfolder of your experiment folder.
Here is an exemple of a home made acquisition for the Ethyl Benzene reference tube (pdf)